电子计价秤示值误差测量结果不确定度评定

本文介绍ACS-15电子计价秤示值误差测量结果不确定度的评定方法,并通过实际测量,计算出7.5kg秤量点的标准不确定度、合成标准不确定度及扩展不确定度。     

Review on synthesis of porous TiO2-based catalysts for energy conversion systems

Porous TiO₂-based catalysts have recently received remarkable attention in the field of energy conversion systems, including hydrogen/oxygen evolution reaction, oxygen/nitrogen reduction reaction, and photodegradation of pollutants owing to their unique structure, large surface area, and good chemical stability. In this report, we review existing research on porous TiO₂-based catalysts for energy conversion systems during the past four years. First, the advantages of porous TiO₂-based catalysts are introduced. Next, the synthetic approaches in developing porous TiO₂-based catalysts are summarized. The different types of energy conversion systems based on porous TiO₂-based catalysts are then presented. Finally, the challenges and future perspectives in synthesizing porous TiO₂-based catalysts are discussed.     

The resolution of analogue measuring devices and its associated uncertainty: An investigation with practical recommendations

Despite the popularity of the analogue measuring devices, there is no recognized reference provided comprehensive guidelines for determining their resolution and its associated uncertainty. For filling this gap, this article is introduced as an attempt to explore and investigate all the available works related to this issue. The new terminology “evident space”, “evident resolution”, and “conjunction” were proposed to set a common reference. Two different techniques for determining the analogue resolution were presented and discussed. Several numerical examples were also presented to show different analogue indications and their interpretations. Moreover, reasonable recommendations for determining the resolution uncertainty were suggested depending on the case.     

Comparison of discriminability of common food acceptance scales for the elderly

This study was aimed to compare four commonly used methods for evaluating consumer acceptance (the 5-point and the 9-point hedonic scales) and preference (the ranking scale and the best-worst scaling) in terms of their ability in discriminating samples and perceived ease of use by the elderly. Elderly (n = 100) and young adult (n = 100) consumers participated in this study. Each consumer evaluated five commercial orange juice samples in duplicate for hedonic rating and preference rank separately and then evaluated ten sets of three samples for the best-worst scale, following the balanced incomplete block design. Nonparametric tests were employed as normality of data was violated. A significant sample effect was observed in all four methods (P < .001). Discriminating power of the best-worst scaling was more pronounced in the elderly than in the young adults; however, the best-worst scaling was easy to use for the young adults than for the elderly.     

负压吸引技术应用于大面积烧伤患者围术期的效果探究

目的:探究环磷酸腺苷联合负压吸引技术应用于大面积烧伤患者围术期的效果及肾保护作用探究。方法:选择2018年12月到2020年12月于医院治疗的120例大面积烧伤患者为研究对象,以随机数字表法对患者分组,60例患者为研究组,60例患者为对照组,对照组给予负压吸引技术治疗,研究组在此基础上给予环磷酸腺苷治疗,治疗前、后测定两组患者干扰素-γ(IFN-γ)、白细胞介素-2(IL-2)、白细胞介素-10(IL-0)、白细胞介素-6(IL-6)、可溶性血管细胞粘附分子-1(sVCAM-1)、一氧化氮(NO)、内皮素(ET-1)、血管内皮生长因子(VEGF)、胱抑素C(Cys-C)、肌酐(Scr)、血尿素氮(BUN)、肾损伤分子-1(KIM-1)水平,记录两组患者手术时间、麻醉苏醒时间、住院时间。结果:研究组IFN-γ、IL-6水平低于对照组(P<0.05),研究组患者IL-2、IL-10水平高于对照组(P<0.05),研究组NO、VEGF水平高于对照组(P<0.05),研究组患者sVCAM-1、ET-1水平低于对照组(P<0.05),研究组患者Cys-C、Scr、BUN、KIM-1水平低于对照组(P<0.05),研究组手术时间低于对照组(P>0.05),研究组麻醉苏醒时间、住院时间低于对照组(P<0.05)。结论:环磷酸腺苷联合负压吸引技术应用于大面积烧伤围术期患者,可降低患者IFN-γ、IL-6水平,提升患者IL-2、IL-10水平,抑制患者炎症,改善患者血管内皮功能,降低患者Cys-C、Scr、BUN、KIM-1水平,减少患者肾功能损伤,减少患者麻醉苏醒时间及住院时间。     

Nickel hydroxide armour promoted CoP nanowires for alkaline hydrogen evolution at large current density

The development of hydrogen evolution activity (HER) electrocatalyst that can run durably and efficiently under the large current density is of special significance but still challengeable for the massive production of hydrogen. Herein, a CoP/Ni(OH)₂ nanowire catalysts grown on Co foam (CF) with a three-dimensional heterojunction structure has been successfully prepared by electrodepositing nickel hydroxide on the surface of cobalt phosphide. The prepared CoP/Ni(OH)₂–15 min sample reveals a superior HER activity and stability. It merely requires ultralow overpotentials of 108 and 175 mV to 100 and 500 mA cm^?2, respectively. In addition, the long-term stability test shows that the catalyst (CoP/Ni(OH)₂–15 min) can operate stably for at least 70 h at 400 mA cm^?2. Utilizing NiFe-LDH/IF with high OER activity, the NiFe-LDH/IF || CoP/Ni(OH)₂–15 min catalyst system possesses the same outstanding performance for overall water splitting (OWS), which can accomplish ≈ 500 mA cm^?2 at 1.74 V in 1 M KOH electrolyte. Moreover, the NiFe-LDH/IF || CoP/Ni(OH)₂–15 min couple can work for more than 80 h at 500 mA cm^?2, indicating its a great prospect in the area of electrolysis water. Such excellent catalytic performance is mainly attributed to the armor effect of Ni(OH)₂, which can not only promote the rapid decomposition of water molecules, but also prevent the loss of phosphorus and enhance the synergistic effect of CoP and Ni(OH)₂. This work can offer a significant reference for the design with high-performance and durable transition metal phosphide electrocatalysts.     

STUDY ON SIMULATION EXPERIMENT OF EQUIVALENT MATERIAL APPLIED IN COAL MINE

IntreductionSimulationexperimentofequivalentmaterialaboutundergroundpressurewasfoundedbYr.H.KySHeuoB(Russian)inthe194o's,andwasintroducedintoourcoalschoolsandresearchinstitutionsinthe196o's.Ithasbeenanexperimentmethodwidelyappliedinlargeengineeringproblemresearchsincethe198o's.Itsadvantageisthatitcandirectlyperceiverockstratafractureandmovementbymineralextraction,thatitisconvenienttodirectlysurveyover1yingrockstratadisplacementandloadtransfer,andobserveitsmovementandbalancelaw.Themoldinclud…     

软弱岩层中大断面硐室施工与支护技术研究

针对姑山铁矿和睦山矿区-300m水平井底车场中央变电所硐室围岩具有松散、软弱和破碎的特点，以软岩巷道支护理论为基础，提出了大断面硐室合理的支护结构与施工方法，简要分析了实现硐室稳定的支护机理，提出初次支护采用锚网喷与低预应力锚索支护，而二次支护采用锚注全断面支护，形成复合锚固支护结构，给出了硐室结构的具体支护参数和施工工艺。应用和现场监测结果表明，由初次锚网喷与锚索和二次锚注组成的复合支护结构满足了软岩地层中大断面硐室的支护要求，取得较好的技术与经济效果。     

特厚坚硬高瓦斯大断面综放切眼锚网锚索耦合支护实践

根据现场工程地质条件调查分析、岩石物理力学特性和特厚坚硬高瓦斯大断面综放切眼围岩力学变形机制及其转化研究,提出了特厚坚硬高瓦斯综放工作面巷道锚网锚索耦合支护设计方案。根据试验结果,证明在白芨沟矿采用锚网锚索耦合支护技术在技术上是可行的、安全上是可靠的、经济上是合理的。